A novel technique for material analysis combines resonant X-ray diffraction and solid-state nuclear magnetic resonance. The researchers at Tokyo Tech have uncovered the previously unknown chemical order of Mo and Nb atoms in the disordered compound Ba7Nb4MoO20. This achievement was made possible by
. This achievement was made possible by utilizing advanced techniques like resonant X-ray diffraction and solid-state nuclear magnetic resonance. The findings of this study highlight the impact that a material’s hidden chemical order can have on its properties, such as ionic conduction. These results are hoped to drive significant advances in the fields of materials science and engineering.
Uncovering the precise structure of a crystalline solid is a difficult task. The properties of materials, including ionic conductivity and chemical stability, are greatly impacted by the chemical order and disorder. However, the techniques that scientists typically use to elucidate unknown crystal structures suffer from serious limitations.
For instance, X-ray and neutron diffraction methods are powerful techniques to reveal the atomic positions and arrangement in the crystal lattice. However, they may not be adequate for distinguishing different atomicInfographic describing the research. Credit: Professor Masatomo Yashima of Tokyo Institute of Technology
To tackle this issue, a research team led by Professor Masatomo Yashima of the Tokyo Institute of Technology in Japan sought to develop a novel and more powerful approach to analyze the order and disorder in crystals. They combined four different techniques to analyze the crystal structure of an important ionic conductor, Ba
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